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  1. #1
    Join Date
    Nov 2011
    Location
    Riverina NSW
    Posts
    211

    Default Epoxy filler alternatives

    I'm building a goat island skiff at the moment and last week exhausted my bucket of fillet/glue powder. There's no commercial fillers locally, or within a few hours. The only option is to order online and wait but with a weekend looming and the need to get gunwales on I went to search old threads here and elsewhere and do research on alternatives. There was mention of fillers like limestone which I could get but nowhere near the fine consistency needed.

    Despite all the recommendations I didn't see any tests performed so I decided to test some of the remaining powder I had left with a couple of alternatives that are often mentioned and that I had on hand, ie wheat flour and wood dust.

    I'll say from the outset that whilst views differ I can appreciate the way my commercial filler held a consistent mix with the epoxy compared to the other two. Despite the flour and dust working I can see that a lot more testing and experience has gone into making commercial mixes. And lastly, whilst I had my doubts when people say wood dust isn't wood flour, I think they're right. I thought my wood flour was pretty darn fine, gathered from particles settled above my dust collectors separator, not the bag. It felt finer than sanding dust from 320g on a random orbital. But the smoothness isn't there like the filler or the wheat flour. Though it can be smoothed prior to curing with a methylated spirits soaked rag and a gloved hand.

    But for this particular test I just wanted to test glue strength rather than filleting, to see if parts pulled apart would separate wood fibres rather than separate along the glue line. The mix was roughly 40/60 by loose volume of epoxy and filler respectively.

    Wood dust, fillet/glue powder, wheat flour
    WP_20160129_14_02_53_Pro.jpg

    From top left counterclockwise; wood dust, wheat flour, fillet/glue powder and top right is wheat flour/wood dust mix. 19mm thick vic ash and 6mm marine ply.
    WP_20160129_14_09_57_Pro.jpg

    Within minutes it was evident at the sides of the fillets that the wood dust and wheat flour experiences loss of epoxy from the mixes as epoxy drains into the substrate.
    WP_20160129_16_17_26_Pro.jpg

    Compared to the fillet/glue powder on the left which shows far less epoxy creeping into the ply around the border of the fillet. The flour/dust mix on the right was the same as above.
    WP_20160129_16_17_35_Pro.jpg

    The destructive tests.
    All fillets were removed prior to the epoxy curing and spring clamps the only clamping force. Curing time was 23hours and temp was warm.
    The ply was cut and clamped to a bench so the vic ash faced down. Holding on to the vic ash I leaned down till the pieces separated.

    Commercial filler. I was expecting a bit more destruction to be honest, though there is fibres in the epoxy.
    WP_20160130_15_29_50_Pro.jpg

    Wood dust. A bit more dramatic.
    WP_20160130_15_31_52_Pro.jpg

    Wheat flour. Removed wood and ply too though there are gum veins in the vic ash
    WP_20160130_15_30_37_Pro.jpg

    Wood and wheat, worked well too.
    WP_20160130_15_32_24_Pro.jpg

    To conclude, there's a few flaws here. I should have waited longer for the epoxy to cure. It was impossible to tell which join was easiest or hardest to break as they all took reasonable force to separate. Despite the the marine ply being uniform I didn't realise there were variances like gum veins in some of the vic ash.

    The commercial filler produces a homogeneous mix that stays that way. The wood dust and flour would separate slowly so after mixing, despite thickness, the mixes would be less viscous down the bottom of a mixing container. In practical use the photo below shows a bit of squeeze out on the glue line whereby the mix used was a wood/wheat mix yet the squeeze out is nearly transparent.
    WP_20160202_01_13_22_Pro.jpg

    For the record the gunwales went on a couple of days ago with a wheat/wood mix and clamps came off today. If it fails I'll let you know. I've finished the major glue ups but will be buying more powder when I'm close to running out of epoxy. I'm still thinking of using wood and wheat for filleting though.
    WP_20160203_10_53_03_Pro.jpg

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  3. #2
    Join Date
    Feb 2008
    Location
    Eustis, FL, USA
    Posts
    2,270

    Default

    I'd like to see you repeat the tests, though this time with appropriate and fair procedures. I've done quite a bit of testing and now don't recommend wood dust at all and wood flour (big difference in particle size), unless it's a non-oily hardwood (very finely ground).

    As to the tests, some of the resin ran out, simply because the joints faying surfaces weren't "primed" before the addition of thickened goo. The test coupons should have been wetted out with straight resin first, so the wood wouldn't suck out the bonding resin from the thickened epoxy, when applied. This would have mitigated a lot of the "resin starvation" you noticed.

    The problem with wood dust and to a lesser degree cooking flour (wheat, rice, corn, etc.) is the particulate size is too big. This is especially true of wood dust, like that from a sander or even as in your case, from the dust collection bag. What happens is the exotherm reaction, thins down the resin and it tends to run out of the joint (or to the bottom of the vertical portion of a fillet). This leaves you with a resin rich bottom and a resin starved top joint/fillet.

    All glue, fillet, fair compound mixtures will have multiple combinations of materials. For example, West System 405 (a filleting mix) is silica, cotton flock, a pinch of talc and a pinch of wood flour. The wood flour is for color, the talc to smooth out the mix, the flock to add a very fibrous, interlocking material and silica to control viscosity.

    There's no one material that can make a good whatever, though some can be used alone, it's usually best if used in combination with other materials. As a rule, silica is a thixotropic agent, which simply means it's used to control viscosity. Used alone, as many folks do, it is strong, stiff and tough, but also tends to make the cured matrix brittle and hasn't any "interlock" or interwoven fibers (like the rebar used in a concrete slab), to insure it can transmit loading forces, within the cured mass.

    In a nutshell, there are three types of mix categories: a heavy structural, a light structural and a cosmetic mix. Both of the structural mixes will need a high fibrous content (milled fibers, flock, 'glass, polyester, stone, metal, etc.), maybe something to ease sanding effort (talc, etc.), though this isn't entirely necessary and of course some silica, so the mix will stay where you put it, depending on application. A cosmetic mix will have light materials (Q-cells, micro spheres, etc.) with a smoothing agent (talc) and again, enough silica to stiffen it up for the application.

    With destructive testing I now use a load cell, but I used to simply use a fish scale. If the sample coupons are small enough, a small scale is all you'll need. Record the testing with video, so you can see the point of failure, which is used for comparative purposes. The key is to do them all the same, with standardized procedures. An example would be the amount of goo used in each joint. I use a notched plastic applicator, specially cut to make uniform 1/16" thick, 1" wide smears of goo. It's just a single 1/16" tall, 1" wide cut in the applicator, with a guide on each edge to hold the plastic off the surface, as I smear goo on the surface. This means each joint has the same amount of goo and the test isn't tossed off, because one joint had a significant difference in glue mass. I also cut the test coupons from the same piece of wood, which are all cut to the same size. The testing rig, holds each piece the same way, with the same "purchase" in the jaws, etc. I also do a "base line" test with each destruction run. This is how I discovered that the use of fillers in epoxy, actually weakens it to some degree. For example, a straight silica fillet has a slight decrease in compressive strength, a modest increase in modulus, but a significant decrease in tension and peel resistance, compaired to a straight resin application. In other words, filler materials alter the physical properties, of straight resin to some degree. Some add a little of something, while detracting in other areas. I found this to be surprising, but it makes sense from a physical/chemical standpoint.

  4. #3
    Join Date
    Nov 2011
    Location
    Riverina NSW
    Posts
    211

    Default

    Hi PAR, great read thanks for the reply. I haven't been ignoring you, rather pondering whether to redo the test. I was in a hurry to see if the wood dust and or flour would work well enough to hold gunwales on, which so far all's well, though we'll have to wait over time to see if there's any long term failure. I've used the dust/flour mix to glue on inwale spacers yesterday and will do the same for the inwales and knees later today but all framing and chinelogs were with the powder. I should add, cost was not a factor in choosing an alternative, it was purely lack of ready supply of the commercial stuff and time running out before I have to go back to work. The major structural stuff has been done with powder and it was just these few items to go before gluing's finished. The 4Litre bucket of powder could've lasted for the whole build but I've wasted so much, which is to be expected when I'm fairly new to this I suppose.

    Regarding priming, I agree, though the thought never occurred until it was too late . Remembering advice about precoating endgrain I did precoat the bow end of gunwales that meet but never thought to wet out bare ply prior to gluing. The ply I've got, although sanded, isn't a finish sand of course and well you can see how resin was sucked away in canyons, so to speak. I wondered whether I'd be left with glue starved or dry joints. For my gunwales at least there's just so much surface area glued I assume it'll be ok. I've come a long way in trusting epoxy. I put screws everywhere in my canoe but none in the GIS, so far.

    I wish I did a straight resin test against the others and have some sort of scale to test against. I've read similar to what you wrote regarding mixes and compromises plus straight epoxy, additions that add features to the thickened epoxy and so forth and how straight epoxy is strong. It does all make sense. I would love to try some microspheres on cosmetic fillets for it's ease in sanding, but also demonstrate on a scale why they shouldn't be used for gluing.

    I'm not sure if I want to put effort into doing another test under stricter conditions,yet, I wont say never. I'm still curious and I'm not sure anyone's shown pictures or demonstrated differences before visually. None that I could find a few days ago. Although I do remember watching in the past a Matthias Wandel youtube video or two where he performed great demonstrations on a home made test rig on adhesives namely different PVA glues, super glues versus fasteners and I'm sure he threw some straight epoxy in one as well. Just a shame he's not into boat building.

  5. #4
    Join Date
    Feb 2008
    Location
    Eustis, FL, USA
    Posts
    2,270

    Default

    I'm a big fan of Matthias Wandel's efforts, though some of his conclusions about PVA's and epoxy aren't consistent with known testing, he's usually anal enough to get things right.

    Testing is pretty common with boat builders, because we need light, yet strong structures, which requires dependance on glued joint performance. This assumes you'll be doing a lot of "goo work". For one boat build, you can just muddle through, likely with few issues, but if you're afflicted with the illness, you'll need to know the realities. The testing permits you to trust goo, but more importantly allows you to setup procedures that you can have faith in, with repeatable results. This is probably the biggest thing with epoxy in general and glues specifically. How tall to make a fillet and what materials to use in it, for a particular application, will help you know how much goo to mix up, how to mix it and how to apply it so it does what it needs to do. For example, after testing (many years worth) I now have premixed jars of fillers; a light structural mix, a heavy structural mix, a cosmedic mix and also mixes specific for different substrates (wood to wood, metal to wood, metal to metal, metal to 'glass, etc.). This way I can just grab the one I need, dump some in the goo and get started, usually with only a pinch of silica to control viscosity for the particular application.

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