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  1. #1
    Join Date
    Feb 2006
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    Perth
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    Default Dispersed Oil Particle generator

    When testing various bits and pieces of dust extraction gear for how efficiently they remove dust I usually use the background dust levels in a shed as the source of dust, and for example measure before and after filtration. However this method has problems.

    Often there is simply not enough dust to perform reliable measurements, especially for large particle sizes, so sometimes I just have to wait until suitable dust levels are around eg burning off days or when inside the house and testing things like masks I wait until SWMBO decided to grill some lamb chops. In the shed I am loathe to run machinery to deliberately fill the shed up with wood dust and this too has problems as its difficult to generate a constant stream of very fine wood dust without making kgs of coarse dust. Large particles also fall out of suspension quicker and change the profile of the particle distribution. High concentrations of wood dust can also choke a particle counter and damage it beyond repair.

    In my electronics area I have used incense sticks but I don't especially like the smell, obtaining s constant stream is not that easy as they don't last very long, and if I use too many they leave a filthy great layer of crap all over the place. Plus the residue is gummy and I don't want too much this stuff inside my particle counters.

    Pro level devices know as Dispersed Oil Particulate (DOP) generators are available for $$$. These generate abundant streams of very fine particles at a constant rate. Usually they use a special oil dropped into an hot chamber that partially vaporises the oil forming a a swarm of fine, mostly invisible 0.25 - 1 micron droplets. These particles are swept by a carrier gas (CO2 or N2) out of the camber and last long enough in the air for the particles to be moved in/through high volume air flow and filtration systems. The drops that are filtered out or pass through the filters or particle counters eventually evaporate away leaving nothing behind.

    Anyway after avoiding this issue for many years I have decided to have a crack at making a small version of a DOP machine and here it is

    The chamber is inside a 1.7kg 65mm long 65mm diameter Brass Hex block to which are attached various SS BSP fittings
    S = is an old 80W soldering iron - eventually this will have some sort of heating control
    OR = is the oil reservoir and there is a needle valve under it for fine control of the oil flow .
    I = the inlet from a small aquarium pump
    O = is the outlet to which another small hose is attached and used to direct the particles to where ever is desired.
    The gauge is a temp gauge from an old BBQ - it reads about 10º to low - all I need it for is to tell me when its up to Temp.
    Guts.jpg

    It takes about 20 minutes to get up to temp but I hope that time can be shorted by insulating the block.

    After placing one drop of oil inside the chamber its looks like very little smoke is being emitted (see below - remember most is invisible) but this amount is more than enough to send my particle counters close to max.
    By photographing the emissions agains a black surface with side lighting its is possible to see the bigger particles.

    Wehaveliftoff.jpg

    The next step is to add adjustable carrier air flow rate and temperature control and explore withe these do.

    There's not a lot to it but a short WIP is in the MW forums here
    Insulating a small heat exchanger - Page 2

    And before anyone elses suggests it no I will not be using it with any other type of hallucinatory oil
    Attached Images Attached Images

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  3. #2
    Join Date
    Jan 2014
    Location
    Sydney Upper North Shore
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    Default

    We use similar to find leaks in vehicle Inlet systems and door seals etc.

  4. #3
    Join Date
    Feb 2015
    Location
    Indiana, US
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    46

    Default

    Interesting concept. Does a liquid particle act the same as a dust particle.
    ? I would think there are significant differences in shape and surface tension.

  5. #4
    Join Date
    Feb 2006
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    Perth
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    Default

    Quote Originally Posted by Maple71 View Post
    Interesting concept. Does a liquid particle act the same as a dust particle.
    ? I would think there are significant differences in shape and surface tension.
    The DOP (Dispersed Oil Particulate) method of generating submicron test particles for super fine filter testing has been around for many decades, certainly from when I started working in labs in the 1970s when yearly DOP tests were performed on our HEPA filters. One of the drivers for DOP testing was to test HEPA filters used in labs and manufacturing involving radiative materials (ie bomb manufacture!) where they had to be super careful about what was let through the filters.

    There are some differences between solid and liquid particles, but for the life time of the test (a few minutes) liquid drops are considered OK plus they have other advantages.

    The first thing to note is we're referring to very fine (mainly 0.2 to 1 microns) and so like regular dust will tend to ride the air flows so if the "openings" in the filter are large enough, the oil liquid drops rarely touch the filter media and go straight through the holes. If the oil drop hits the filter material they usually stick but to a great extent so will dust particles. The A in HEPA stands for (high efficiency particulate) ARRESTANCE. Small dust particles ride the air flow until the strike the filter media and are impacted or partially buried in the mat of filter fibres rather than bounce off the fibres. This is what makes it difficult to efficiently clean superfine filters and they are usually replaced. To protect these filters from becoming quickly blocked by large particles a coarse pre-filter or lower efficiency (and cheaper) HEPA is used. The HEPA filters in our labs lasted about 7-8 years, but some in our ultra clean labs lasted for 20+ years.

    The beauty of the DOP test is, if the right oil is used and the filter fans are run continuously after the test the oil droplets eventually evaporate away and so not permanently clog the filters. Some of our filters were DOP tested every year for 20 years without any problems.

  6. #5
    Join Date
    Feb 2006
    Location
    Perth
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    Default

    Update to DOP generator.

    Insulated with 4 layers of material from an old fibreglass fire blanket.
    Heat shield cladding made from stainless from an old clothes dryer drum.
    "Glass and Brass" Oil reservoir - yes that is a neck from a wine bottle

    Jacketed.jpg

    Now just waiting for some heat resistant Locktite (272) to seal the threads to arrive before I can fire it up.

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